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We report the first simultaneous, common‐volume lidar observations of thermosphere‐ionosphere Fe (TIFe) and Na (TINa) layers in Antarctica. We also report the observational discovery of nearly one‐to‐one correspondence between TIFe and aurora activity, enhanced ionization layers, and converging electric fields. Distinctive TIFe layers have a peak density of ~384 cm⁻³and the TIFe mixing ratio peaks around 123 km, ~5 times the mesospheric layer maximum. All evidence shows that Fe⁺ion‐neutralization is the major formation mechanism of TIFe layers. The TINa mixing ratio often exhibits a broad peak at TIFe altitudes, providing evidence for in situ production via Na⁺neutralization. However, the tenuous TINa layers persist long beyond TIFe disappearance and reveal gravity wave perturbations, suggesting a dynamic background of neutral Na, but not Fe, above 110 km. The striking differences between distinct TIFe and diffuse TINa suggest differential transport between Fe and Na, possibly due to mass separation.

We report on the relationship between a pulsating aurora and a relativistic electron microburst using simultaneous observations of ground‐based fast auroral imagers with the FIREBIRD‐Ⅱ CubeSat for the first time. We conducted a detailed analysis of an event on October 8, 2018 and found that the occurrence of the pulsating aurora with internal modulations corresponds to the flux enhancement of electrons with energy ranging from ∼220 keV to >1 MeV detected with Flight Unit 4, one of FIREBIRD's CubeSat, with a time delay of ∼585 ms. Combining of this time delay result and time of flight model, we suggest that the pulsating aurora and the microburst occur simultaneously due to the chorus waves at different latitudes along the same field‐line as predicted by Miyoshi et al. (2020,https://doi.org/10.1029/2020gl090360).